Synthesis of ZnO Nanoparticles by a Novel Surfactant Assisted Amine Combustion Method

Prabhu, Yendrapati Taraka and Rao, Kalagadda Venkateswara and Kumar, Vemula Sesha Sai and Kumari, Bandla Siva (2013) Synthesis of ZnO Nanoparticles by a Novel Surfactant Assisted Amine Combustion Method. Advances in Nanoparticles, 02 (01). pp. 45-50. ISSN 2169-0510

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Abstract

The as precursor, HMTA as fuel material and non-ionic surfactant (Triton-X 100). The X-Ray diffraction (XRD) analysis revealed that the synthesized ZnO nanopowder has the pure wurtzite structure. The ZnO powder shows polycrystalline nature having the crystallite size 21.25 nm. Crystallite size is calculated using Debye-Scherrer’s and Williamson-Hall equations. Porosity, Cell Volume, Micro strain, Morphology Index, Lorentz factor and Lorentz Polarization factor are also studied. From differential thermal analysis (DTA) & thermo gravimetric (TGA) it has been confirmed that nano powder has the phase purity. The weight loss percentage of the sample is 2.8385%. The particle size obtained 29 nm is in good agreement with the crystallite size calculated from X-Ray Diffraction pattern with the Particle Size Analyzer. The morphology of as prepared Zinc oxide nanopowders are characterized by scanning electron microscope (SEM). From specific area electron diffraction (SAED) pattern has specified the d-spacing and corresponding planes which coincide with the XRD d-spacing and planes.

Item Type: Article
Subjects: West Bengal Archive > Medical Science
Depositing User: Unnamed user with email support@westbengalarchive.com
Date Deposited: 01 Jun 2023 08:24
Last Modified: 02 Sep 2024 12:41
URI: http://article.stmacademicwriting.com/id/eprint/929

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